Full Utilization of Lignocellulose with Ionic Liquid Polyoxometalates in a One-Pot Three-Step Conversion.
Identifieur interne : 000961 ( Main/Exploration ); précédent : 000960; suivant : 000962Full Utilization of Lignocellulose with Ionic Liquid Polyoxometalates in a One-Pot Three-Step Conversion.
Auteurs : Yiming Li [République populaire de Chine] ; Xueyan Zhang [République populaire de Chine] ; Zonghang Li [République populaire de Chine] ; Jiaying Song [République populaire de Chine] ; Xiaohong Wang [République populaire de Chine]Source :
- ChemSusChem [ 1864-564X ] ; 2019.
Abstract
The lignin-first concept is a new innovation for full utilization of lignocellulose into value-added chemicals. Ionic liquid (IL) polyoxometalates [MIMPS]2 H4 P2 Mo18 O62 [MIMPS=1-(3-sulfonic group) propyl-3-methyl imidazolium] are reported to be active in the cleavage of β-O-4, α-O-4, and 4-O-5 bonds in three kinds of lignin models and also efficient for converting native lignocellulose. The three components in soft or hard lignocellulose were depolymerized in a one-pot three-step treatment. For soft lignocellulose (pine), lignin was first decomposed into guaiacol and phenol with yields of 15.3 and 12.9 % at 98.6 % delignification efficiency at 130 °C for 14 h. Meanwhile, hemicellulose and cellulose were intact during the delignifying process and were subsequently hydrolyzed to 3.5 % xylose at 100 % hemicellulose conversion efficiency at 150 °C for 14 h and 36.4 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h, respectively. For hard lignocellulose (poplar), the yields of guaiacol and phenol were 10.1 and 8.7 % at 91.9 % delignification efficiency at 130 °C for 14 h, whereas 12.9 % xylose at 90.4 % hemicellulose conversion efficiency at 150 °C for 12 h and 32.9 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h were obtained. [MIMPS]2 H4 P2 Mo18 O62 achieved the full utilization of lignocellulose with total conversion in the lignin-first strategy and also showed the easy separation as a result of temperature-reversibility with ten recycling runs.
DOI: 10.1002/cssc.201902503
PubMed: 31532070
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China.</nlm:affiliation><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024</wicri:regionArea><wicri:noRegion>130024</wicri:noRegion></affiliation></author><author><name sortKey="Zhang, Xueyan" sort="Zhang, Xueyan" uniqKey="Zhang X" first="Xueyan" last="Zhang">Xueyan Zhang</name><affiliation wicri:level="1"><nlm:affiliation>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024, P.R. China.</nlm:affiliation><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024</wicri:regionArea><wicri:noRegion>130024</wicri:noRegion></affiliation></author><author><name sortKey="Li, Zonghang" sort="Li, Zonghang" uniqKey="Li Z" first="Zonghang" last="Li">Zonghang Li</name><affiliation wicri:level="1"><nlm:affiliation>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024, P.R. China.</nlm:affiliation><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024</wicri:regionArea><wicri:noRegion>130024</wicri:noRegion></affiliation></author><author><name sortKey="Song, Jiaying" sort="Song, Jiaying" uniqKey="Song J" first="Jiaying" last="Song">Jiaying Song</name><affiliation wicri:level="1"><nlm:affiliation>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024, P.R. China.</nlm:affiliation><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024</wicri:regionArea><wicri:noRegion>130024</wicri:noRegion></affiliation></author><author><name sortKey="Wang, Xiaohong" sort="Wang, Xiaohong" uniqKey="Wang X" first="Xiaohong" last="Wang">Xiaohong Wang</name><affiliation wicri:level="1"><nlm:affiliation>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024, P.R. China.</nlm:affiliation><country xml:lang="fr" wicri:curation="lc">République populaire de Chine</country><wicri:regionArea>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024</wicri:regionArea><wicri:noRegion>130024</wicri:noRegion></affiliation></author></analytic><series><title level="j">ChemSusChem</title><idno type="eISSN">1864-564X</idno><imprint><date when="2019" type="published">2019</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The lignin-first concept is a new innovation for full utilization of lignocellulose into value-added chemicals. Ionic liquid (IL) polyoxometalates [MIMPS]<sub>2</sub> H<sub>4</sub> P<sub>2</sub> Mo<sub>18</sub> O<sub>62</sub> [MIMPS=1-(3-sulfonic group) propyl-3-methyl imidazolium] are reported to be active in the cleavage of β-O-4, α-O-4, and 4-O-5 bonds in three kinds of lignin models and also efficient for converting native lignocellulose. The three components in soft or hard lignocellulose were depolymerized in a one-pot three-step treatment. For soft lignocellulose (pine), lignin was first decomposed into guaiacol and phenol with yields of 15.3 and 12.9 % at 98.6 % delignification efficiency at 130 °C for 14 h. Meanwhile, hemicellulose and cellulose were intact during the delignifying process and were subsequently hydrolyzed to 3.5 % xylose at 100 % hemicellulose conversion efficiency at 150 °C for 14 h and 36.4 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h, respectively. For hard lignocellulose (poplar), the yields of guaiacol and phenol were 10.1 and 8.7 % at 91.9 % delignification efficiency at 130 °C for 14 h, whereas 12.9 % xylose at 90.4 % hemicellulose conversion efficiency at 150 °C for 12 h and 32.9 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h were obtained. [MIMPS]<sub>2</sub> H<sub>4</sub> P<sub>2</sub> Mo<sub>18</sub> O<sub>62</sub> achieved the full utilization of lignocellulose with total conversion in the lignin-first strategy and also showed the easy separation as a result of temperature-reversibility with ten recycling runs.</div></front></TEI><pubmed><MedlineCitation Status="PubMed-not-MEDLINE" Owner="NLM"><PMID Version="1">31532070</PMID><DateCompleted><Year>2019</Year><Month>11</Month><Day>25</Day></DateCompleted><DateRevised><Year>2020</Year><Month>01</Month><Day>08</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1864-564X</ISSN><JournalIssue CitedMedium="Internet"><Volume>12</Volume><Issue>22</Issue><PubDate><Year>2019</Year><Month>Nov</Month><Day>22</Day></PubDate></JournalIssue><Title>ChemSusChem</Title><ISOAbbreviation>ChemSusChem</ISOAbbreviation></Journal><ArticleTitle>Full Utilization of Lignocellulose with Ionic Liquid Polyoxometalates in a One-Pot Three-Step Conversion.</ArticleTitle><Pagination><MedlinePgn>4936-4945</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1002/cssc.201902503</ELocationID><Abstract><AbstractText>The lignin-first concept is a new innovation for full utilization of lignocellulose into value-added chemicals. Ionic liquid (IL) polyoxometalates [MIMPS]<sub>2</sub> H<sub>4</sub> P<sub>2</sub> Mo<sub>18</sub> O<sub>62</sub> [MIMPS=1-(3-sulfonic group) propyl-3-methyl imidazolium] are reported to be active in the cleavage of β-O-4, α-O-4, and 4-O-5 bonds in three kinds of lignin models and also efficient for converting native lignocellulose. The three components in soft or hard lignocellulose were depolymerized in a one-pot three-step treatment. For soft lignocellulose (pine), lignin was first decomposed into guaiacol and phenol with yields of 15.3 and 12.9 % at 98.6 % delignification efficiency at 130 °C for 14 h. Meanwhile, hemicellulose and cellulose were intact during the delignifying process and were subsequently hydrolyzed to 3.5 % xylose at 100 % hemicellulose conversion efficiency at 150 °C for 14 h and 36.4 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h, respectively. For hard lignocellulose (poplar), the yields of guaiacol and phenol were 10.1 and 8.7 % at 91.9 % delignification efficiency at 130 °C for 14 h, whereas 12.9 % xylose at 90.4 % hemicellulose conversion efficiency at 150 °C for 12 h and 32.9 % glucose at 100 % cellulose conversion efficiency at 170 °C for 12 h were obtained. [MIMPS]<sub>2</sub> H<sub>4</sub> P<sub>2</sub> Mo<sub>18</sub> O<sub>62</sub> achieved the full utilization of lignocellulose with total conversion in the lignin-first strategy and also showed the easy separation as a result of temperature-reversibility with ten recycling runs.</AbstractText><CopyrightInformation>© 2019 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.</CopyrightInformation></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Li</LastName><ForeName>Yiming</ForeName><Initials>Y</Initials><AffiliationInfo><Affiliation>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024, P.R. China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Zhang</LastName><ForeName>Xueyan</ForeName><Initials>X</Initials><AffiliationInfo><Affiliation>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024, P.R. China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Li</LastName><ForeName>Zonghang</ForeName><Initials>Z</Initials><AffiliationInfo><Affiliation>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024, P.R. China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Song</LastName><ForeName>Jiaying</ForeName><Initials>J</Initials><AffiliationInfo><Affiliation>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024, P.R. China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Wang</LastName><ForeName>Xiaohong</ForeName><Initials>X</Initials><Identifier Source="ORCID">http://orcid.org/0000-0001-8465-9782</Identifier><AffiliationInfo><Affiliation>Key Lab of Polyoxometalate Science of Ministry of Education, Faculty of Chemistry, Northeast Normal University, Changchun, 130024, P.R. China.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><GrantList CompleteYN="Y"><Grant><GrantID>51578119</GrantID><Agency>National Natural Science Foundation of China</Agency><Country></Country></Grant><Grant><GrantID>20180414069GH</GrantID><Agency>Jilin Provincial Science and Technology Department</Agency><Country></Country></Grant></GrantList><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2019</Year><Month>10</Month><Day>22</Day></ArticleDate></Article><MedlineJournalInfo><Country>Germany</Country><MedlineTA>ChemSusChem</MedlineTA><NlmUniqueID>101319536</NlmUniqueID><ISSNLinking>1864-5631</ISSNLinking></MedlineJournalInfo><CitationSubset>IM</CitationSubset><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">biomass</Keyword><Keyword MajorTopicYN="N">ionic liquids</Keyword><Keyword MajorTopicYN="N">lignin</Keyword><Keyword MajorTopicYN="N">lignocellulose</Keyword><Keyword MajorTopicYN="N">polyoxometalates</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2019</Year><Month>09</Month><Day>11</Day></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2019</Year><Month>9</Month><Day>19</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2019</Year><Month>9</Month><Day>19</Day><Hour>6</Hour><Minute>1</Minute></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2019</Year><Month>9</Month><Day>19</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate></History><PublicationStatus>ppublish</PublicationStatus><ArticleIdList><ArticleId IdType="pubmed">31532070</ArticleId><ArticleId IdType="doi">10.1002/cssc.201902503</ArticleId></ArticleIdList><ReferenceList><Reference><Citation>G. 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Hallett, Green Chem. 2019, 21, 692-703.</Citation></Reference></ReferenceList></PubmedData></pubmed><affiliations><list><country><li>République populaire de Chine</li></country></list><tree><country name="République populaire de Chine"><noRegion><name sortKey="Li, Yiming" sort="Li, Yiming" uniqKey="Li Y" first="Yiming" last="Li">Yiming Li</name></noRegion><name sortKey="Li, Zonghang" sort="Li, Zonghang" uniqKey="Li Z" first="Zonghang" last="Li">Zonghang Li</name><name sortKey="Song, Jiaying" sort="Song, Jiaying" uniqKey="Song J" first="Jiaying" last="Song">Jiaying Song</name><name sortKey="Wang, Xiaohong" sort="Wang, Xiaohong" uniqKey="Wang X" first="Xiaohong" last="Wang">Xiaohong Wang</name><name sortKey="Zhang, Xueyan" sort="Zhang, Xueyan" uniqKey="Zhang X" first="Xueyan" last="Zhang">Xueyan Zhang</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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